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Crystal structure and thermal chemical properties of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane

X. M. Li, C. F. Ding, B. Q. Tian, Q. Liu, S. S. Zhang, H. Xu, and P. K. Ouyang

College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao, 266042, P. R. China

 

E-mail: shushzhang@126.com

Received: 13 April 2005  Revised: 27 February 2006  Accepted: 8 March 2006

Abstract: The crystal structure of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane has been determined by single crystal X-ray diffraction method. The crystal belongs to triclinic system, space group P-1 with unit cell constants a = 11.2877(9) Å, b = 11.9539(9) Å, c = 12.2365(9) Å, α = 97.2580(10)°, β = 116.2850(10)°, γ = 106.3710(10)°, V = 1358.48(18) Å 3, Z = 2, D c = 1.234 g/cm3, μ = 0.079 mm−1, F(000) = 536, R and w(R) are 0.0718 and 0.2055, respectively, for 5239 unique reflections with 3745 observed reflections (I > 2σ(I)).

Keywords: synthesis - crystal structure - fluorine - thermal chemical properties

Full paper is available at www.springerlink.com.

DOI: 10.2478/s11696-006-0039-3

 

Chemical Papers 60 (3) 220–223 (2006)

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