ISSN print edition: 0366-6352
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Preparation, Spectral and Thermal Properties of Dicyanoargentates of Copper and Nickel with Bipyridine

J. Chomič, J. Černák, and M. Bálintová

aDepartment of Inorganic Chemistry, Faculty of Science, P. J. Šafárik University, SK-041 54 Košice

 

E-mail: chomic@kosice.upjs.sk

Received: 22 January 2001

Abstract: Coordination compounds [Ni(bipy)3]2[Ag(CN)2]3Cl · 9H2O (NB3AH), [Ni(bipy)2][Ag(CN)2]2 · H2O (NB2AH), and [Cu(bipy)2][Ag(CN)2]2 ·H2O (CB2AH), respectively, have been prepared and identified by elemental analysis, infrared and electron spectroscopy. Thermal stability and stoichiometry of thermal decomposition were studied by using a derivatograph. The intermediates of thermal decomposition were identified by IR spectroscopy and X-ray powder diffractometry. The results indicate that the thermal stability increases in the order NB3AH, CB2AH, NB2AH.

Full paper in Portable Document Format: 562a84.pdf

 

Chemical Papers 56 (2) 84–88 (2002)

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