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Preparation of O-(3-azido-2-hydroxypropyl)cellulose and its photolysis to O-(2-formyl-2-hydroxyethyl)cellulose

L. Petruš and M. Petrušová

Institute of Chemistry, Centre for Chemical Research, Slovak Academy of Sciences, CS-842 38 Bratislava

 

Abstract: 0-(3-Azido-2-hydroxypropyl)cellulose has been prepared by the reaction of 0-(3-chloro-2-hydroxypropyl)cellulose with sodium azide in dimethyl sulfoxide. Photolysis of this compound in 2-methoxyethanol and subsequent acid hydrolysis afforded 0-(2-formyl-2-hydroxyethyl)cellulose.

Full paper in Portable Document Format: 404a519.pdf

 

Chemical Papers 40 (4) 519–522 (1986)

Wednesday, April 24, 2024

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