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Photolysis of 1-azido-1-deoxyalditols preparation of D-mannose

M. Petrušová, M. Fedoroňko, and L. Petruš

Institute of Chemistry, Centre for Chemical Research, Slovak Academy of Sciences, CS-842 38 Bratislava

 

Abstract: 3,4- O-Isopropylidene-1 - 0-(4-methylbenzenesulfonyl)-D-mannitol has been prepared by partial tosylation of the starting 3,4-O-isopropylidene-D-man-nitol. This derivative was treated with sodium azide to give 1-azido-l-deoxy-3,4-0-isopropylidene-D-mannitol, which on photolysis and subse­quent acid hydrolysis afforded D-mannose.

Full paper in Portable Document Format: 405a655.pdf

 

Chemical Papers 40 (5) 655–658 (1986)

Thursday, April 18, 2024

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