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Preparation of S-[2,3-bis(ethylthio)maleimidomethyl] thio- and -dithiophosphates, their spectral and biological properties

F. Gregáň, V. Konečný, and J. Kmec

Department of Inorganic and Organic Chemistry, Faculty of Pharmacy, Komenský University, 832 32 Bratislava

 

Abstract: Sixteen S-[2,3-bis(ethylthio)maleimidomethyl] thio- and -dithiophosphates I (R = alkyl; R1 = alkoxy, Ph, Me2N; Z = O, S) were prepd. from N-(bromomethyl)-2,3-bis(ethylthio)maleimide and K salts of organophosphorus acids. IR, UV and 1H NMR spectra were measured. A linear relationship was found between ν(P = O) and Σσ* of the P substituents; the effect of the medium on the splitting of the absorption band ν(P = O) was studied. The prepd. compds. were tested for insecticidal, acaricidal, ovicidal, and fungicidal activities.

Full paper in Portable Document Format: 364a547.pdf

 

Chemical Papers 36 (4) 547–557 (1982)

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