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Reactions of arenecarbonyl isothiocyanates with hydrazones

M. Uher, M. Bošanský, Š. Kováč, and O. Rajniaková

Department of Organic Chemistry, Slovak Technical University, 880 37 Bratislava

 

Abstract:  By the reaction of benzoyl and 2-furoyl isothiocyanates, respectively, with acetone phenylhydrazone 5-benzoylimino- and 5-(2-furoylimino)-2,2-di- methyl-4-phenyl-l,3,4-thiadiazolines, respectively, were formed. The reaction with benzaldehyde phenylhydrazone resulted in benzaldehyde 2-phe- nyl-4-acylthiosemicarbazones, while that with acetophenone and ben- zophenone phenylhydrazones, respectively, did not proceed at all. The u.v., i.r., mass, 1H-n.m.r., and 13C-n.m.r. spectra are discussed.

Full paper in Portable Document Format: 355a707.pdf

 

Chemical Papers 35 (5) 707–712 (1981)

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