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Rapid solidification processing in molten salts chemistry: X-ray analysis of deeply undercooled cryolite-alumina melts

Michal Korenko, Marián Kucharík, and Dušan Janičkovič

Institute of Inorganic Chemistry, Slovak Academy of Sciences, Dúbravská cesta 9, SK-845 36 Bratislava, Slovak Republic

 

E-mail: uachmiko@savba.sk

Received: 20 June 2007  Revised: 8 August 2007  Accepted: 13 September 2007

Abstract: Rapid solidification processing (cooling rate from the interval 105–106 K s−1) was used to prepare deeply undercooled cryolite-alumina melts. Such prepared samples were analyzed by the XRD method. Besides cryolite, XRD patterns belonging to ι-Al2O3 were recorded. The influence of annealing on the XRD patterns of deeply undercooled melts was also investigated.

Keywords: rapid solidification processing - cryolite-alumina melt - XRD - deeply undercooled melts

Full paper is available at www.springerlink.com.

DOI: 10.2478/s11696-008-0014-2

 

Chemical Papers 62 (2) 219–222 (2008)

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