ISSN print edition: 0366-6352
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Determination of aromatic amines by the method of direct injection enthalpimetry

M. Šťastný, J. Vulterin, R. Volf, and P. Maršolek

Department of Analytical Chemistry, Institute of Chemical Technology, 166 28 Prague

 

Abstract: An enthalpimetric detn. of arom. amines based on the diazotization and nitrosation reaction heats was developed. This detn. was verified with 7 selected amines, i.e. sulfanilic acid, p-aminobenzoic acid, aniline, o-toluidine, α-naphthylamine, benzidine, and Ph2NH. The method of double injection, esp. suited for high values of reaction heats was applied.

Full paper in Portable Document Format: 333a410.pdf

 

Chemical Papers 33 (3) 410–419 (1979)

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