ISSN print edition: 0366-6352 ISSN electronic edition: 1336-9075 Registr. No.: MK SR 9/7 Published monthly

Reactions of 4-substituted cinnamoyl isothiocyanates with 1-phenoxy-2,3-epoxypropane and sodium hydrogen selenide

M. Dzurilla and P. Kristián

Department of Organic Chemistry, Faculty of Natural Sciences, P. J. Šafárik University, 041 67 Košice

Abstract:  The synthesis of 2-(4-X-rinnamóylimino)-5-phenoxymethyl-l,3-oxathiolanes and 6-(4-X-phenyl)-2-thioxo-4-oxoperhydro-l,3-selenazines by cyclization of 4-substituted cinnamoyl isothiocyanates with l-phenoxy-2,3-epoxypropane and sodium hydrogen selenide, respectively, is described. The structures of the nine synthesized compounds were proved by i.r. and ¹H-n.m.r. spectroscopy.

Full paper in Portable Document Format: 336a792.pdf

Chemical Papers 33 (6) 792–797 (1979)