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Alternative syntheses of methylated sugars. XV. Chemical synthesis of methyl β-xylobioside

P. Kováč, J. Hirsch, and V. Kováčik

Institute of Chemistry, Slovak Academy of Sciences, 809 33 Bratislava

 

Abstract: Condensation of 2,3,4-tri-O-acetyl-1-bromo-1-deoxy-α-D-xylopyranose with Me 2,3-anhydro-β-D-ribopyranoside afforded Me 2,3-anhydro-4-O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-β-D-ribopyranoside. Its deacetylation followed by treatment with aq. KOH gave Me β-xylobioside.

Full paper in Portable Document Format: 324a514.pdf

 

Chemical Papers 32 (4) 514–518 (1978)

Tuesday, June 18, 2024

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