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Synthesis of 2-deoxy-α-D-glucopyranosyl and 2-deoxy-α-D-galactopyranosyl phosphates

Š. Kučár, J. Zámocký, and Š. Bauer

Institute of Chemistry, Slovak Academy of Sciences, 809 33 Bratislava

 

Abstract:  2-Deoxy-α -D-glucopyranosyl and 2-deoxy-α -D-galactopyranosyl phosphates have been prepared by phosphorylation of 1,3,4,6-tetra-O-acetyl-2-deoxy-α -D-glucopyranose and l,3,4,6-tetra-0-acetyl-2-deoxy-α -D-galactopyranose with crystalline H3PO4. Acetylation of 2-deoxysugars introduced by Bonner has been applied in the synthesis of crystalline 1,3,4,6-tetra-O-acetyl-2-deoxy-α-D-galactopyranose.

Full paper in Portable Document Format: 281a115.pdf

 

Chemical Papers 28 (1) 115–119 (1974)

Tuesday, August 09, 2022

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