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Stabilization of daughter 99mTc after the ß-decay of 99Mo in dihydrido-bis(cyclopentadienyl)molybdenum-(99Mo)

V. Mikulaj, F. Macášek, and R. Kopunec

Department of Nuclear Chemistry, Faculty of Natural Sciences, Komenský University, 801 00 Bratislava

 

Abstract: The chem. forms were studied of the stabilization of 99mTc following the β-decay of 99Mo in (C5H5)299MoH2. 99mTc was stabilized in high yield in the form (C5H5)299mTcH (I). Sublimation with a temp. gradient and paper chromatog. were used for the sepn. of I if the 99Mo decayed in the cryst. state. The yield of I was 88 ± 2% by sublimation and 94 ± 4% by paper chromatog. If the decay occurred in benzene the yield of I as detd. by paper chromatog. was 79 ± 3%. If the decay occurred in 3N-HCl the yield was estd. to be 78% by benzene extn.

Full paper in Portable Document Format: 271a23.pdf

 

Chemical Papers 27 (1) 23–31 (1973)

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