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Furan Derivatives. XXX. Preparation of Substituted 5-Phenyl-2-furfuryl Alcohols

R. Frimm, A. Krutošíiková, and J. Kováč

Department of Organic Chemistry, Slovak Technical University, Bratislava 1

 

Abstract: The preparation of 5-(X-phenyl)-2-furfuryl alcohols from the corresponding aldehydes is described by a) reduction with NaBH4 , when X = 2-N02, 3-N02, and 4-N02 ; b) reduction with LiAlH4, when X = 2-Cl, 3-Cl, 4-Cl, 4-Br, 4-CH3, 4-OCH3, H; c) modified Cannizzaro reaction, when X = 2-N02, 3-N02, 4-N02 , 4-CH3, 4-OCH3, H. Infrared and ultraviolet spectra of the final products are interpreted.

Full paper in Portable Document Format: 266a551.pdf

 

Chemical Papers 26 (6) 551–556 (1972)

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