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The Crystal and Molecular Structure Analysis of the Centrosymmetric Polynuclear Ferrocene Complex (C10H9Fe)3C(C4OH7)

F. Hanic, J. Ševčík, and E. L. McGandy

Institute of Inorganic Chemistry, Slovak Academy of Sciences, Bratislava 9

 

Abstract:  The crystal and molecular structure of the polynuclear ferrocene complex   (C10H9Fe)3C(C4OH7) has been explained by X-ray structure analysis using direct methods. The space group symmetry is PI. The asymmetric part of the unit cell contains two molecules (C10H9Fe)3C(C4OH7). The polynuclear molecules consist of three ferrocenyl groups bonded to the common carbon atom. The fourth group bonded to the same carbon atom is a tetrahydrofuran ring. The ring atoms of ths cyclopentadiene rings do not deviate significantly from planarity. The angle of tilt between the least-squares planes is between 2.9° to 8.9°. The diffractometric intensities of 2292 independent reflections have been used. The final R factor was 0.063.

Full paper in Portable Document Format: 242a81.pdf

 

Chemical Papers 24 (2) 81–106 (1970)

Monday, June 17, 2024

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