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Procedures for Preparation of Sealed Powder Patterns and Single Crystal Samples for X-Ray Diffraction Methods in Controlled Atmosphere without Dry Box

M. Zikmund and A. Valent

Institute of Inorganic Chemistry, Slovak Academy of Sciences, Bratislava 9

 

Abstract: In the present paper device and procedures are described for preparation of flat powdered samples of air-sensitive substances in an inert atmosphere without the application of a dry box. The samples are to be submitted to measurements with X-ray diffractograph and with the Guinier method. Further a method for filling single crystals into capillary tubes of Lindemann glass for measurements with the Weissenberg method are reported.

Full paper in Portable Document Format: 2311-12a934.pdf

 

Chemical Papers 23 (11-12) 934–937 (1969)

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