ISSN print edition: 0366-6352
ISSN electronic edition: 1336-9075
Registr. No.: MK SR 9/7
Procedures for Preparation of Sealed Powder Patterns and Single
Crystal Samples for X-Ray Diffraction Methods in Controlled
Atmosphere without Dry Box
M. Zikmund and A. Valent
Institute of Inorganic Chemistry, Slovak Academy of Sciences,
Abstract: In the present paper device and procedures are described for preparation
of flat powdered samples of air-sensitive substances in an inert atmosphere
without the application of a dry box. The samples are to be submitted to
measurements with X-ray diffractograph and with the Guinier method.
Further a method for filling single crystals into capillary tubes of Lindemann
glass for measurements with the Weissenberg method are reported.
Full paper in Portable Document Format: 2311-12a934.pdf
Chemical Papers 23 (11-12) 934–937 (1969)