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Gas chromatography of trimethylsilyl ethers of some 17-oxo steroids

D. Podhradský and M. Š. Kandráč

Research Laboratory, Department of Internal Medicine, Medical Faculty, University of P. J, Šafárik, Košice

 

Abstract: Trimethylsilyl ethers of 17-ketosteroids were separated by gas chromatography through the use of NGS, and QF-1 phases. Relative retention times found in the mentioned phases with innert supports Chromosorb W, and Gas Chrom Q are compared. Advantages, and an availability of described phases for the separation of 17-ketosteroids occuring in human urine are discussed.

Full paper in Portable Document Format: 233a224.pdf

 

Chemical Papers 23 (3) 224–228 (1969)

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