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Simultaneous preparation of 4,6-dinitro-3-methylphenol and 2,4-dinitro-3-methylphenol

I. Pastorek

Forschungsinstitut für agrochemische Technologie, Bratislava

 

Abstract: It was detd. that the nitration of 4-nitro-3-methylphenol forms not only 4,6-dinitro-3-methylphenol (I) but also 2,4-dinitro-3-methylphenol (II). On the basis that I, m. 74°, is sol. in cold C6H6 and II, m. 133°, is sol. in boiling C6H6 and very slightly sol. in cold C6H6, I and II were sepd. and isolated.

Full paper in Portable Document Format: 195a420.pdf (in Slovak)

 

Chemical Papers 19 (5) 420–421 (1965)

Wednesday, June 26, 2019

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