ISSN print edition: 0366-6352
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Determination of silicon in O-(trimethylsilyl) derivatives of saccharides

V. Bílik, I. Ježo, and Ľ. Stankovič

Slovak Academy of Sciences, Bratislava

 

Abstract: Si in some O-(trimethylsilyl) saccharides, O-(trimethylsilyl) polyols, (trimethylsilyl) amines, and trimethylsilyl esters of org. acids is detd. by hydrolysis of the sample to yield trimethylsilanol and hexamethyldisiloxane. The latter are swept by a stream of O into a combustion tube, where they are burned to SiO2.

Full paper in Portable Document Format: 189a688.pdf (in Slovak)

 

Chemical Papers 18 (9) 688–691 (1964)

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