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Space group of symmetry of p-dimethylaminophenyl isothiocyanate and 4-[bis(β-chloroethyl)amino]phenyl isothiocyanate

L. Ulický and T. Dillingerová

Slovak Technical University, Bratislava

 

Abstract: cf. CA 58, 10812d. Both compds. crystallize in the triclinic system, probable space group ̅P. p-Me2NC6H4-NCS has a 10.00, b 22.62, c 17.72 A., α 147°, β 43° 50', γ 152°; pycnometer d. = 1.12, Z = 3. p-(ClCH2CH2)2NC6H4NCS has a 29.31, b 6.60, c 6.69 A., α 92° 40', β 100°, γ 92° 30'; pycnometer d. = 1.72; Z = 4. From mol. dimensions, calcd. on basis of ion radii, a symmetrical arrangement of 2 head-to-tail pairs of parallel planar mols. is assumed for the 2nd compd.

Full paper in Portable Document Format: 177a493.pdf (in Slovak)

 

Chemical Papers 17 (7) 493–497 (1963)

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