ISSN print edition: 0366-6352
ISSN electronic edition: 1336-9075
Registr. No.: MK SR 9/7
Preparation of p-iodophenyl isothiocyanate labeled with sulfur-35 and iodine-131
P. J. Safarik University, Košice
Abstract: A new method for the prepn. of p-IC6H4NCS (I) labeled with131I by isotopic ion-exchange with Na I131 was described. The specific activity of I was small. For the prepn. of I tagged with 35S and 131I of high sp. activity, a direct iodination of aniline with 131I and thiophosgenation of p-iodoaniline with CS35SCl2 was applied. Double labeled I is pure, suitable for biol. activity, and sol. in olive oil.
Full paper in Portable Document Format: 161-2a60.pdf (in Slovak)
Chemical Papers 16 (1-2) 60–64 (1962)