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Preparation of p-iodophenyl isothiocyanate labeled with sulfur-35 and iodine-131

M.Zaduban

P. J. Safarik University, KoŇ°ice

 

Abstract: A new method for the prepn. of p-IC6H4NCS (I) labeled with131I by isotopic ion-exchange with Na I131 was described. The specific activity of I was small. For the prepn. of I tagged with 35S  and  131I of high sp. activity, a direct iodination of aniline with 131I and thiophosgenation of p-iodoaniline with CS35SCl2 was applied. Double labeled I is pure, suitable for biol. activity, and sol. in olive oil.

Full paper in Portable Document Format: 161-2a60.pdf (in Slovak)

 

Chemical Papers 16 (1-2) 60–64 (1962)

Wednesday, November 13, 2019

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