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Some complex salts of beryllium and organic acids

Ľ. Krasnec and J. Krätsmár-Šmogrovič

Slovak University, Bratislava

 

Abstract: Complex Be salts of the type Be4O(RCO2)6 are prepd. by dissolving Be(OH)2 in boiling alc. soln. of org. acids according to 4Be(OH)2 + 6RCO2H = Be4O(RCO2)6 + 7H2O. BzOH gives Be4O(C6H5CO2)6 (I), m. 316-7°, identical with the basic Be benzoate described in the literature. I with 2-thiophenecarboxylic acid gives Be4O(C4H3SCO2)6, m. 391-2°; with 2-furancarboxylic acid, Be4O(C4H3OCO2)6, m. 368-70°; with ο-O2NC6H4CO2H, Be4O(ο-O2NC6H4CO2)6, m. 279-80°; with m-O2NC6H4CO2H, Be4O(m-O2NC6H4CO2)6, m. 378-80°; with p-O2NC6H4CO2H, Be4O(p-O2NC6H4CO2)6, m. 410-12°.

Full paper in Portable Document Format: 77a421.pdf (in Slovak)

 

Chemical Papers 7 (7) 421–428 (1953)

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