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Three-component one-pot reaction for the synthesis of β-amide ketones

Yan-Ping Luo and Qiong Chen

Key Laboratory of Protection and Development Utilisation of Tropical Crop Germplasm Resources, Hainan University, Ministry of Education, HaiKou, 570228, China

 

E-mail: yanpluo@yahoo.com.cn

Abstract: β-amide ketones were synthesised by a three-component one-pot reaction of phenylacetylene, aldehydes, and amides in anhydrous acetonitrile containing trifluoroacetic acid and acetic acid in the presence of AlCl3 catalyst. The title compound structures were identified by 1H NMR, 13C NMR, MS, and elemental analysis.

Keywords: β-amide ketones – one-pot reaction – synthesis

Full paper is available at www.springerlink.com.

DOI: 10.2478/s11696-013-0313-0

 

Chemical Papers 67 (5) 532–537 (2013)

Wednesday, May 22, 2024

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