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Reaction of 2,4-Dichlorophenylglyoxyjhydroximoyl Chloride with Amines as a Convenient Method for the Synthesis of Amide Oximes and Amides

L. Jarošková and Ľ. Fišera

Department of Organic Chemistry, Faculty of Chemical Technology, Slovak Technical University, SK-812 37 Bratislava

 

Abstract: 2,4-Dichlorobenzoylnitrile oxide (I) generated in situ from the title compound reacts with amines under the condition of 1,3-dipolar cycloaddition to afford the amide oximes IV and amides V. The ratio of IV and V depends on the structure of amine. Reaction of I with cyclic amines gave only IV. The reaction mechanism is briefly discussed.

Full paper in Portable Document Format: 481a31.pdf

 

Chemical Papers 48 (1) 31–34 (1994)

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